Inficon HAPSITE Smart Plus Chemical Identification System Uživatelský manuál

OPERATING MANUALHAPSITE® Smart PlusChemical Identification SystemIPN 074-472-P1C

CE Implementation Date: October 2004 Authorized Representative: Duane H. Wright Operations Quality Manager, ISS INFICON Inc.

3 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.1.1 Emergency Mode (EMER MODE)In an emergency, the concentrator cleanout can be bypassed

3 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3 A confirmation message will be displayed. Touch Yes or push OK SEL to continue. See Figure

3 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 To take the system out of Emergency Mode, touch the EMER MODE button. Alternately, use the

3 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2 Touch Concentrator Cleanout or highlight Concentrator Cleanout using the arrow keys. Push O

3 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4 When the cleanout is successful, the Concentrator Cleanout Succeeded message will be disp

3 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2 Touch Skip Cleanout or highlight Skip Cleanout using the arrow keys. Push OK SEL. See Figu

3 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4 The HAPSITE will re-run the cleanout as part of its preparation.5 If the failure box appe

3 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.2 Selecting a Different Method Using the SELECT METHOD IconIf the default method is not t

3 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 The SYSTEM IS NOT READY screen will appear. To select a new method, touch SELECT METHOD o

3 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 The PREPARING message will again be displayed. See Figure 3-25. Refer to steps 4-9 of Sect

WARRANTY AND LIABILITY - LIMITATION: Seller warrants the products manufactured by it, or by an affiliated company and sold by it, and described on the

3 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.2.1 Changing the Default MethodThe default method for the HAPSITE can be changed. By cha

3 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.2.2 Show AllThe HAPSITE will only show methods that are compatible with the current sampl

3 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualProcedure1 If an Analyze method is going to be run after Survey, verify that the appropriat

3 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 Using the touch screen, touch RUN SURVEY. See Figure 3-32.Figure 3-32 Survey Ready6 Alter

3 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8 Sample air away from the point of concern for one minute. Remember to note the background

3 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating Manual10 By touching CMPD ID, a list of identified compounds will appear. See Figure 3-37. The CAS

3 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual12 To view the chromatogram while the method is running, touch GRAPH. See Figure 3-39. Alte

3 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating Manual14 To confirm the Survey results with a GC/MS run, ANALYZE can be touched or ANALYZE RUN can

3 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.3.1 Quick Reference SOP — Survey Method1 If you are running an Analyze (GC/MS) method af

3 - 25IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.4 ANALYZE (GC/MS) Mode with the Concentrator3.4.1 The Tri- Bed ConcentratorThe Tri-Bed c

3 - 26 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4 Using the touch screen, touch RUN ANALYZE. See Figure 3-43.Figure 3-43 Analyze Button5 A

3 - 27IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 3-45 Collecting Sample For Concentrator RunCAUTIONDo not touch the sample with the p

3 - 28 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8 By touching CMPD ID, a list of found compounds will appear. See Figure 3-47. This page wi

3 - 29IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 3-48 Sample Chromatogram View For Concentrator10 A METHOD FINISHED message will appe

3 - 30 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.4.4 Quick Reference SOP—Concentrator Methods1 Verify that the concentrator is installed.

3 - 31IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.5 Detecting Hazardous ChemicalsIf the compound identification turns red, a chemical’s con

3 - 32 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.5.1 View Results/View ReportsData files and reports can be viewed from the main front pa

3 - 33IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3 The most recent file for the selected method will appear on the screen. Use the black, tou

3 - 34 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 Scroll through the method files and highlight the desired method. Either touch Select or

3 - 35IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7 Touch the small blue triangles to display the compound identification and retention time f

IPN 074-472-P1CHAPSITE Smart Plus Operating ManualDefinition ofNote, Hint, Danger, Warning and Caution ParagraphsNOTE: This is a note paragraph. Note

3 - 36 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9 A link to the NIOSH Pocket Guide to Chemical Hazards (NPG) will also be displayed in blue

3 - 37IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11 Touching the CMPD ID (Compound Identification) button while in Review Results, will show

3 - 38 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual12 Touching a specific compound in the list will display that compound’s NIOSH database inf

3 - 39IPN 074-472-P1CHAPSITE Smart Plus Operating Manual14 To view the Summary, Qualitative and Quantitative Reports, touch the REPORTS button. Alte

3 - 40 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual16 The Qualitative Report can be found be touching the QUAL button. See Figure 3-66. Altern

3 - 41IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 3-68 Type of Method

3 - 42 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.6 The Help IconThe Help icon is located on the upper right of the front panel. See Figur

3 - 43IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.7 The Info IconThe Info icon is located on the upper right of the front panel. See Figure

3 - 44 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual1 An important resource on this database is The NIOSH Pocket Guide to Chemical Hazards (NPG

3 - 45IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2 When the publication appears, touch INDEX with CHEMICAL NAMES and SYNONYMS. See Figure 3-7

IPN 074-472-P1C HAPSITE Smart Plus Operating ManualOperating Manual Style ConventionsThe following information describes the conventions used through

3 - 46 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Scroll down to display an alphabet. Touch the first letter of the desired compound. See F

3 - 47IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 Touch the desired chemical. The Pocket Guide for that specific chemical will be displayed.

3 - 48 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7 To access information regarding Immediately Dangerous to Life or Health Concentrations (I

3 - 49IPN 074-472-P1CHAPSITE Smart Plus Operating Manual9 Scroll down, press DOWN or use the down arrow to find the desired compound. Touch the link

3 - 50 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.7.1 System ParametersSystem Parameters provides information about the operation of the H

3 - 51IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.7.1.1 Battery IconIf a battery is installed, the Battery icon will display information ab

3 - 52 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.7.1.3 Internal Standard IconThe Internal Standard icon uses a vertical bar graph to corr

3 - 53IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.7.1.4.1 HEATERS ButtonTouching the HEATERS icon provides the current temperatures of the

3 - 54 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.7.1.4.3 CONC ButtonInformation about the concentrator can be found through this button.

3 - 55IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.7.1.5 TUNE STATUS IconThis icon provides information about the state of the HAPSITE’s tun

TOC - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualTable Of ContentsTrademarksDefinition of Note, Hint, Danger, Warning and Caution Paragraphs

3 - 56 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.7.1.5.1 TUNE REPORTSWhen the TUNE STATUS icon has been touched, see Figure 3-92, a butto

3 - 57IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.7.1.6 GPS IconThe GPS icon will displays the latitude and longitude coordinates of the HA

3 - 58 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.7.1.7.1 HAPS ButtonThe HAPS button will provide the HAPSITE name, the HAPSITE’s Serial N

3 - 59IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.7.1.7.3 DATE TIME ButtonThis button displays the present date and time. See Figure 3-98.F

3 - 60 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.7.2 AccessoriesThe Accessories icon will display information regarding the current confi

3 - 61IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.8 EXIT MenuThe EXIT menu is located on the top row of the front panel. See Figure 3-101.

3 - 62 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4 For Turn Off, the screen will become dark and the HAPSITE will turn off the power.4a For

3 - 63IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.8.1 Extended StandbyExtended Standby is the preferred mode for storing the HAPSITE during

3 - 64 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Alternately, touch EXIT or use the arrow keys to highlight EXIT. Push OK SEL. See Figure

3 - 65IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 3-107 Confirming Standby Option6 The HAPSITE will go into Extended Standby. Remove t

TOC - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.4.6.2 Connect Laptop with Wireless Connection. . . . . . . . . . . . . . . . . . . . . .

3 - 66 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.8.1.1 End Standby1 To End Standby, touch END STANDBY or using the arrow keys, highlight

3 - 67IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.9 Analyze (GC/MS) Mode with Headspace Sampling System in Portable ModeThe Headspace Sampl

3 - 68 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 When powered on or taken out of Extended Standby, the HAPSITE will automatically start pr

3 - 69IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 3-113 Collecting Sample11 The next screen will prompt Sampling is Done. Again, no ac

3 - 70 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual12a The CMPD ID screen can also be accessed by using the arrow keys to highlight CMPD ID an

3 - 71IPN 074-472-P1CHAPSITE Smart Plus Operating Manual14 At the end of the Headspace run, a prompt will appear. When prompted Insert needle into a

3 - 72 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.9.1 Quick Reference SOP — GC/MS Mode with HSS in Portable Mode1 Verify that the desired

3 - 73IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.10 SituProbeFor complete information on SituProbe methods, see Chapter 14, SituProbe. For

3 - 74 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8 Using the touch screen, touch RUN ANALYZE. If using the push buttons, push ANALYZE RUN.Fi

3 - 75IPN 074-472-P1CHAPSITE Smart Plus Operating Manual10 The next screen will prompt Sampling is Done. See Figure 3-122. Again, no action is requi

TOC - 3IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 3Operating HAPSITE in Portable Mode3.1 Starting the HAPSITE in Portable Mode. . . .

3 - 76 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual12 To view the chromatogram while the method is running, touch GRAPH. Alternately, use the

3 - 77IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3.10.2 Quick Reference SOP — GC/MS Mode with SituProbe in Portable Mode1 Verify that the de

3 - 78 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

4 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 4Wireless and Touch Screen Options4.1 Wireless Option4.1.1 IntroductionThe HAPSITE

4 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualCAUTIONTo maintain compliance with FCC standards and regulations and to ensure the proper op

4 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4.1.3 Regulatory Compliance Information for CANADIAN UsersThis section of the Operating Manu

4 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis symbol indicates compliance with the essential requirements of Directive 73/23/EEC and

4 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4.1.4.2 European EMC Compliance StatementTable 4-1 Country - RestrictionCountries Restricti

4 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4.1.4.3 European Safety Compliance StatementThis device has been tested and certified accor

4 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4.1.6 Turning On the RadioIf wireless communication is desired, the radio must be turned on.

TOC - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3.7.2 Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

4 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Press the button until a click is heard. The green lights adjacent to “Radio” and “WLAN” s

4 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4.1.7.2 Setting Up Plus IQ for Communication with the HAPSITEThe first step to communication

4 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4.1.8 Wireless Module Indicator LightsLocated on the Wireless Module inside the HAPSITE fr

4 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual1 Open the front panel of the HAPSITE.2 Remove the cover from the power switch (for the wire

4 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4.2 The MAIN MenuThe MAIN menu contains the following options: View Results, Smart Interfa

4 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 4-7 Smart Interface4 The HAPSITE Smart software will be displayed. See Figure 4-8.Fi

4 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4.2.2 Adjust BrightnessThe brightness level of the Touch Screen can be adjusted to make vi

4 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 4-12 Scroll Bar4 To darken the screen, slide the bar to the left. To brighten, slide

4 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual6 To exit the Black Screen mode, push the SYSTEM and HELP Buttons together at the same time

4 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4.3 Touch Screen OptionsNOTE: If the Touch Screen freezes, pushing the MENU and ESC keys at

TOC - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4.4 The USB Drive . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

4 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Touch Calibrate or push OK SEL when Calibrate is highlighted. See Figure 4-18.Figure 4-18

4 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 Instructions on screen calibration will appear. Touch OK or highlight OK and push OK SEL.

4 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7 Touch OK in the next ten seconds if the calibration was accurate for all four targets. Ot

4 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2 From the drop-down menu, touch Touch Screen. Alternately, use the arrow keys to highlight

4 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4.3.2.2 Enabling the Touch Screen1 Using the arrow keys, highlight MAIN and touch OK SEL.

4 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4.4 The USB Drive4.4.1 Copying Files to the USBData files can be saved to the USB drive on

4 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4 Touch the USB icon.Touch Copy to USB or using the arrow keys, highlight Copy to USB and p

4 - 25IPN 074-472-P1CHAPSITE Smart Plus Operating Manual6 Touch the desired file for copying and touch Select. Alternately, use the arrow keys to hi

4 - 26 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8 A bar will be displayed on the screen to show the download’s progress. Touch Close to ret

4 - 27IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4.4.2 Copying Files From the USBThe Copying Files from the USB button can be used to transf

TOC - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7.4 AutoTune Failure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

4 - 28 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4 Touch the USB icon. Touch COPY FROM USB or using the arrow keys, highlight COPY FROM USB

4 - 29IPN 074-472-P1CHAPSITE Smart Plus Operating Manual6 A progress bar will be shown on the screen. Touch Close to return to the USB screen. If an

4 - 30 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4.4.3 Updating the Front Panel Software from the USBPeriodically, there may be updates to

4 - 31IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 Touch the desired update and touch Select. See Figure 4-42NOTE: If there is not an update

4 - 32 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7 The following screen will be displayed while the system is updating. Touch Done to exit t

4 - 33IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4.4.4 Retrieving Files from the USBOnce files have been saved to the USB drive, they can be

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5 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 5Operating HAPSITE in Laptop Mode5.1 Starting the HAPSITE in Laptop ModeStarting the

5 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5.2 Survey ModeThe Survey Mode is used for quick analysis and tentative results. The run pe

5 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4 As part of the HAPSITE’s preparation, it will run AutoTune. If AutoTune successfully runs a

TOC - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual8.9.1 Changing Access Levels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual10 Monitor the Probe distance indicator bar on the HAPSITE screen for guidance. See Figure 5

5 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 5-7 Sample Survey Run Complete13 To view the data, note the data file name and click

5 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5.2.1 Quick Reference SOP — Running Survey Mode1 Either power on the HAPSITE or take the HA

5 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5.3 Selecting a New Method1 Click the Abort button. See Figure 5-9.Figure 5-9 Aborting Meth

5 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Choose a folder that matches the physical configuration of the HAPSITE. In this example th

5 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4 Click the desired method and then click OK. See Figure 5-12Figure 5-12 Selecting the Metho

5 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5.4 Analyze (GC/MS) Mode with LoopThis method is used for analyzing samples with concentra

5 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4 The HAPSITE will check pressures and automatically heat up all necessary zones to the setp

5 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 5-16 Chromatogram in Progress11 Wait for the method to run to completion. Figure 5-

5 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 5-17 Sample Complete 12 Review results at the end of the run.13 To view the data, no

TOC - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9.8.3.1 Accessing NIST from AMDIS . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5.4.1 Quick Reference SOP — Running Analyze (GC/MS) Loop Method1 Verify that the Sample Lo

5 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5.5 Analyze (GC/MS) Mode with Concentrator5.5.1 Tri- Bed ConcentratorThis method is used f

5 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 5-20 AutoTune Complete5 A Concentrator Cleanout will also be run as part of the HAP

5 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating Manual10 When prompted Sampling is Done on the HAPSITE screen, remove the probe from the sample so

5 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualNOTE: If the HAPSITE has been left unattended, the message SYSTEM IS NOT READY may appear.

5 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5.6 Analyze (GC/MS) Mode with Headspace Sampling System The Headspace Sampling System is us

5 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 5-25 Headspace Needle6 When powered on or taken out of Extended Standby (refer to s

5 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating Manual10 A prompt will appear Press RUN to start method.NOTE: The sample must be heated for 20 min

5 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 5-29 Headspace Running a Concentrator Method15 When prompted at the end of the run,

5 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 5-31 HSS Concentrator Method Finished17 To analyze the data, see Chapter 9, Data Rev

TOC - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.6 Tune Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5.6.1 Quick Reference SOP — GC/MS Mode with HSS 1 Double-click the Plus IQ software icon.2

5 - 25IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5.7 SituProbe MethodsSee Chapter 14 for more information on running SituProbe methods.5.7.1

5 - 26 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9 The next screen will prompt Sampling is Done. See Figure 5-33. No action is required by t

5 - 27IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5.7.2 Quick Reference SOP — Analyze Mode with SituProbe1 Double-click the Plus IQ software

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6 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 6Methods6.1 Introduction to MethodsThe versatility of the HAPSITE lies in the variet

6 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualCAUTIONAll unknown samples should first be collected with the Survey Method to estimate the

6 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual6.2.1 Building a Survey Method Library FileSurvey methods can be designed for data collectio

6 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 6-2 Data File Information PageDuring the Calibration run, enter the concentration le

6 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating ManualThe spectrum of the analyte must be recorded to the target compound library. The spectrum is

TOC - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualChapter 13Headspace Sampling System13.1 Introduction. . . . . . . . . . . . . . . . . . .

6 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 6-5 Grab Spectrum for Template WindowThe compound is displayed in the Analytes in Li

6 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 6-6 Additional Calibration PointsAdditional compounds are added by following the same

6 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualCAUTIONAll unknown samples should first be collected with the Survey Method to avoid saturat

7 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 7Tune7.1 Introduction to AutoTune and Manual TuneEnsuring the mass spectrometer (MS)

7 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7.2 AutoTuneThere are two versions of the AutoTune program: Short and Long. The Short AutoT

7 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7.2.1 Starting AutoTune from the Manual Tune Screen on the Laptop Computer1 Double-click on

7 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7.3 Viewing a Tune ReportThe Tune Report can be viewed from the front panel display or from

7 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating ManualTo view the Tune Report from the front panel display, touch the HAPSITE icon and then touch t

7 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7.4 AutoTune FailureOccasionally, AutoTune may fail. Follow the procedures outlined below b

7 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 Select default.tun file and press OK. See Figure 7-10.Figure 7-10 Select "default.tun

TOC - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual14.7.2 Purge . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7 Highlight default.tun. Click OK. See Figure 7-12.NOTE: This will overwrite the default.tun

7 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7.5 Manual Tune Settings and ControlsManual Tune is run from the Laptop computer. The Manual

7 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7.5.1 Tool BarFigure 7-14 Manual Tune Tool BarFilament On/Off . . . . . . . . . Turns th

7 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating ManualShow Bounds . . . . . . . . . . . Displays the peak centroid and the target peak width at 10

7 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualShow Tune Status Panel . . . . . . . . Displays the Tune and Mass Calibration Status panel.

7 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating ManualShow Target . . . . . . . . . . . . . . . . . . Displays the target bar for the mass peak c

7 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7.5.3 Tune Control PanelFigure 7-17 Tune Control PanelThe Tune Control Panel provides acc

7 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating ManualThe Emission button turns the filament ON or OFF, the EM button turns the Electron Multiplie

7 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualMass Cal.. . . . . . . . . . . . . . . . . . . . . Checks and corrects the ten calibration

7 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7.5.4 Peak Scan WindowThe Peak Scan Window, see Figure 7-18, displays the mass peak and ena

TOC - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual15.3.9 Communications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualY Axis Scale . . . . . . . . . . . . . . Increase or decreases the Y axis scale.NOTE: For t

7 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7.5.5 Full Scan WindowThe Full scan window (see Figure 7-19) is used for display purposes t

7 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 7-20 Setting the Full Scan RangeDefault Scan ranges of 45 - 300 AMU or 1 - 45 AMU c

7 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 7-22 Tune and Mass Calibration Status MenuMass . . . . . . . . . . . . . . . . . .

7 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualMax OK Target Percentage . . . . . . Displays the maximum percentage required for the mass

7 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating ManualDiff(mmu) . . . . . . . . . . . . . . . . . . . . Provides an adjustment to DAC value for m

7 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualMass Centered Width. . . . . . . . . . . Width in AMU that correctly aligns the calibration

7 - 25IPN 074-472-P1CHAPSITE Smart Plus Operating ManualNOTE: The menu from the control panel is the same as above with the exception of no print fu

7 - 26 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7.6.1 Adjusting Base Peak Gain1 Double-click on the Plus IQ icon. See Figure 7-27.Figure 7

7 - 27IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 7-30 Checking BPG and EM VoltageFigure 7-31 BPG Low

TOC - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual16.6.2.2 Reactivation Using the Front Panel . . . . . . . . . . . . . . . . . . . . . . .

7 - 28 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5a If yes, then the BPG does not need adjustment. Proceed to Step 8.5b If no, the BPG will

7 - 29IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7.6.2 Adjusting Resolution1 Before adjusting Resolution, Base Peak Gain must be adjusted. R

7 - 30 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 7-34 Target Percentage Low3b If the red box is in the Max Target Percentage, the Ta

7 - 31IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7.6.3 Adjusting the Ion Energy1 Prior to performing this procedure, follow the steps outlin

7 - 32 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 After making Ion Energy adjustments:3a If the red boxes no longer appear, indicating the

7 - 33IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 7-37 Save Tune ButtonFigure 7-38 Tune Saved5 Exit Manual Tune by closing the Tune w

7 - 34 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

8 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 8Plus IQ Software8.1 The HAPSITE Software - Plus IQPlus IQ software includes all of

8 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8.2 Computer System RequirementsThe following is the minimum recommended computer system fo

8 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual8.4 Installing/Updating NIST and AMDISThe NIST and AMDIS mass spectral libraries are powerfu

TOC - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualB.1.1 How to Establish the Desired Concentrations . . . . . . . . . . . . . . . . . . . .

8 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4 The welcome window for the NIST and AMDIS setup will appear. Press Next. See Figure 8-4.Fi

8 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual6 Press Next. Refer to Figure 8-5.7 When prompted to choose the software destination location

8 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9 When prompted to select a program folder, use the default shown in Figure 8-8 and press Ne

8 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual12 The installation will proceed automatically and will last a few minutes. See Figure 8-11.F

8 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8.5 Reloading Default HAPSITE MethodsAll of the default methods are saved on the Laptop. Th

8 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating ManualAir_Tri-Bed_PPB_Standard . . . . . . Basic Carbon Concentrator method (15 minute analysis tim

8 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualNOTE: In addition to the standard 15 minute methods, there are 25 minute methods for the Sa

8 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4 Double-click the Analyze folder for Analyze methods (or Survey folder for a Survey method)

8 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 Double-click on the appropriate folder for the method to be saved. See Figure 8-17.NOTE:

8 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual8.6 Establishing Communications between the HAPSITE and Laptop Computer Establishing commun

1 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 1Introduction1.1 The HAPSITE Smart Plus SystemThe HAPSITE® Smart Plus Portable Gas C

8 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Enter the letter "H", followed by the last 3 or 4 significant digits of the Ser

8 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating Manual8.6.2 Configuring the HAPSITE for Communications1 If communication between the HAPSITE and

8 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4b Click on Connect to, drag the cursor over Show All Connections and click Left Mouse Butt

8 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 The Network Connection Status Window will open. Click the desired connection and press Pro

8 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual6 In the General tab, scroll down and highlight Internet Protocol (TCP/IP), press Propertie

8 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7 Select Use the following IP address and enter the IP address of the HAPSITE, (refer to Ste

8 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8.6.3 Establishing Communication with the Service ModuleService Module communications will

8 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating ManualWhen Add Port is selected, the window shown in Figure 8-31 will appear. Select the appropria

8 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8.7 Establishing Communications between the HAPSITE and Laptop Computer Using the Wireless

8 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4 Select the correct Time Zone from the drop-down list above the map.5 Press OK and reboot t

OPERATING MANUALIPN 074-472-P1CHAPSITE® Smart PlusChemical Identification Systemwww.inficon.com [email protected] ©2008 INFICON

1 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualHeadspace Sampling System . . . Also known as the HSS, the HSS is an accessory to the HAPS

8 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8.9.1 Changing Access LevelsNOTE: When Normal access level is selected, a message will app

8 - 25IPN 074-472-P1CHAPSITE Smart Plus Operating Manual8.9.2 Setting or Changing the Access Level Password1 To change the Advanced level password,

8 - 26 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8.10 Plus IQ ControlsThe System Setup Page is the main screen of the Plus IQ software. The

8 - 27IPN 074-472-P1CHAPSITE Smart Plus Operating Manual8.10.1 System Setup Main MenuThe Main Menu in the System Setup view includes entries which

8 - 28 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8.10.1.4 Tools MenuThe Tools menu, shown in Figure 8-45, is consistent for all screens in

8 - 29IPN 074-472-P1CHAPSITE Smart Plus Operating Manual8.11 Software Versions for the HAPSITE and LaptopHAPSITE Smart Plus’s use HAPSITE Smart Plu

8 - 30 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual8.12 HAPSITE IconsTable 8-2 HAPSITE IconsIcon DescriptionStarts Plus IQ Software from Des

8 - 31IPN 074-472-P1CHAPSITE Smart Plus Operating ManualAllows editing and creating methods.Accesses the Service Module when attached.Accesses HAPSI

8 - 32 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualNavigates through files in Data Review.Navigates through peaks in “search for peaks”.Return

9 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 9Data Review9.1 Introduction to Data Review The Data Review section of the HAPSITE S

1 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating ManualInternal Standards Gas Use-Rate . . . . . . . 1 canister per 24 hours of operation (This depe

9 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9.2 Accessing the Data Review FeatureThe Data Review feature can be accessed as follows: D

9 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating ManualThe Recall window will appear. Select the desired data file, either from the PC or the HAPSIT

9 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 9-4 Sections of the Data Review ScreenTIC/RIC Window . . . . . . . . . . . . . . . T

9 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual9.3 Data Review ToolbarThe Data Review toolbar is shown in Figure 9-5.Figure 9-5 Data Revie

9 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual . . . . . . . . . . . . . . . . . . . . . . . . . Opens AMDIS Program.. . . . . . . . . . .

9 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual9.4 RMB (Right Mouse Button) Menus within Data ReviewAll functions within Data Review can be

9 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualLabel Chromatogram . . . . . . . . . . . Brings up a text box to label the chromatogram. The

9 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual9.4.2 RMB in the Spectrum Display WindowThe Spectrum display is shown in the Scan Window. Ev

9 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualSpectrum Mass List . . . . . . . . . . . . Displays a report of all the masses in the spect

9 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual9.5 The TIC/RIC Display FunctionsThere are tools available to assist in the Data Review pro

1 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manuallibrary (included with the Plus IQ software). See section 9.8, NIST Library Searches, on pag

9 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9.5.2 How to Use Background Subtraction WARNINGBe careful not to subtract a data/peaks tha

9 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual1 Using the Scan Cursor, select a peak of interest in the chromatogram. Refer to Figure 9-10

9 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9.5.2.2 Background Subtraction Using a Range of PointsFigure 9-12 Using Background Subtra

9 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating Manual9.5.2.3 Additional Features of the Background ToolIf the cursor is placed over B1 or B2, an

9 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 9-14 Using the Range Tool9.5.3.1 Steps Required to Range Acquisition1 Place the cu

9 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating Manual9.5.3.2 Additional Features of the Range ToolIf the cursor is placed over R1, and the RMB i

9 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9.6.1 Using the Zoom Function in the TIC/RIC WindowThere are two ways to Zoom into a TIC/R

9 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 9-17 Zoomed Spectrum3 To Unzoom, click on the Magnifying Glass with the "-"

9 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 Place cursor within the desired Zoom area, the cursor will turn into a magnifying glass.

9 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 9-20 RIC PlotWhen the box in the Control Panel labeled -RIC is checked, the TIC/RIC

1 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual1.6 Description Of SubsystemsThe HAPSITE is comprised of the following subsystems: Gas Chro

9 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Enter the name of the compound, to be located, in the box on the top left of the screen.

9 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 9-26 RIC Plot for Suspected Benzene One Mass Selected10 The compound may be present

9 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9.8 NIST Library SearchesA TIC or sequential SIM peak qualitative identification can be ac

9 - 25IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 9-29 Search Results DisplayAdditional information may be obtained by checking the bo

9 - 26 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 9-30 Comparison of NIST and SpectrumIf the Description box is checked, the NIST hea

9 - 27IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 9-31 Peaks Menu ChoicesTo view and adjust the search parameters, select Change Searc

9 - 28 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 9-33 Post Analysis DisplayIn Figure 9-33, both the Search for Peaks function and th

9 - 29IPN 074-472-P1CHAPSITE Smart Plus Operating ManualQualitative identification of each peak found by the Search function can be done by checking

9 - 30 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 9-36 Preview ScreenThe report is displayed, refer to Figure 9-36. Some options are:

9 - 31IPN 074-472-P1CHAPSITE Smart Plus Operating ManualWhen the analyst invokes AMDIS, upon completion of the analysis, the program returns the Res

1 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 1-2 Total Ion ChromatogramThe performance of the column is affected by temperature,

9 - 32 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 9-38 AMDIS Confirm WindowThis window shows the complete analysis, peak by peak. If

9 - 33IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 9-39 NIST Database Search9.8.4 Analyzing Data Using NISTBy right-clicking on the Sp

9 - 34 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualClear NIST Grab file . . . . . . . . . . . . Clears the grab file of previous files.Switch

9 - 35IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 9-42 NIST DatabaseNotice the tabs at the bottom of the NIST window. These are multip

9 - 36 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9.9 Reporting and Printing DataReports are generated in Data Review utilizing the HAPSITE

9 - 37IPN 074-472-P1CHAPSITE Smart Plus Operating ManualSummary . . . . . . . . . . . . . . . . . . . . . Generates a report based upon the Qualitat

9 - 38 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9.10 Plus IQ Hot KeysTable 9-1 Plus IQ Hot KeysKeys FunctionsCrtl+o Open data fileF3 Data

10 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 10Saving and Managing Files10.1 Saving Files on the HAPSITEFile types are created t

10 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 10-1 Save Method File Dialog Window - HAPSITE Option SelectedEnter the new file nam

10 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual10.1.2 Event Log FilesEvent Log Files are created automatically by the system to record sys

1 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating ManualIn the Survey mode of operation, in which air samples are passed directly to the mass spectro

10 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 10-4 Method Editor - Data, Showing File Name OptionsThe system allows flexibility t

10 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating ManualNOTE: Tune files are saved, by default, to the HAPSITE hard drive under the \Tune folder.Fig

10 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 10-7 Save Tune File ScreenOnce the Tune file is saved, the Save Tune File and Manua

10 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual10.1.5 Data ReviewData review is used to view and analyze data files. To open files, double

10 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 10-10 Data Review Recall WindowThe data file is opened in the Data Review window, a

10 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 10-11 Viewing Results in the Data Review WindowData files stored on the Laptop may a

10 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual10.2.1 Method FilesMethod files are created using the HAPSITE Plus IQ software to direct

10 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual10.2.2 Event Log FilesEvent Log Files are created automatically by the system to record sy

10 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual10.2.3 Data FilesData files are automatically saved to the HAPSITE hard drive. Data files

10 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 10-16 Manage Files Dialog WindowIn the Manage Files window, the left side displays

1 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manualthe rods. Once on the rod, the heavier ion is neutralized. At a specific combination of RF a

10 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFiles or folders may be deleted using the Delete button. Select the desired file or folder

11 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 11Method Editor11.1 The Method EditorWARNINGOnly trained users should create method

11 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual The Full Scan component, which defines the mass range and other parameters of the Mass Sp

11 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 11-3 Error Information ButtonThe order of pages that appear in Wizard mode for vario

11 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual11.2 Accessing Method EditorCAUTIONRead all of Chapter 11 before creating a method.NOTE: F

11 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.3 Description PageWARNINGIncorrect selections for the mode of analysis may not identify

11 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualMode of AnalysisAnalyze (GC/MS) . . . . . . . . . . . . . . This analysis uses both the Ga

11 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating ManualMethod elements are: If the HAPSITE is to operate separate from the Service Module, the HAP

11 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual The quantitation sequence method must be defined. This includes the definition of: the D

11 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.4 Startup PageThe Startup Page, shown in Figure 11-7 and Figure 11-8, allows for setting

1 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating ManualThe two vacuum pumps of the HAPSITE continue to provide the pumping necessary for operation.

11 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 11-8 Method Editor Startup Page for Survey MethodsThe parameters on the Startup pa

11 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating ManualProbe . . . . . . . . . . . . . . . . . . . . . . . . The target temperature the Probe must

11 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual11.4.1 HeadspaceWARNINGOnly trained users should create methods. Choosing the incorrect s

11 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.4.2 SituProbeWARNINGOnly trained users should create methods. Choosing the incorrect sa

11 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual11.5 Inlet PageWARNINGOnly trained users should modify methods. Changing parameters may r

11 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 11-12 Method Editor Inlet Page for GC/MS Full ScanThe only difference on the Inlet

11 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 11-13 Inlet Page for Analyze (GC/MS) SIM11.5.1 Inlet StatesWARNINGOnly trained us

11 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating ManualHINT: When editing from the keyboard, the Alt+DownArrow key combination will "pull&quo

11 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 11-15 Valve States for an Inlet State EventFigure 11-16 Customizing the Valve Sta

11 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 11-17 Accessing the Inlet StatesThe following choices are available in the Inlet St

1 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual1.6.4.2 Gas Chromatograph ControlThe Gas Chromatograph control circuitry includes the powe

11 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualBackflush . . . . . . . . . . . . . . . . . . . . This Inlet State sets the GC valves so

11 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating ManualLine Purge. . . . . . . . . . . . . . . . . . . . This Inlet State turns on the sampling pu

11 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualSPConcFill . . . . . . . . . . . . . . . . . . . This sets the GC valves so that the samp

11 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.5.3 Use Internal StandardThe selection to use an Internal Standard is available for Loo

11 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualHINT: In some applications, if the Mass Spectrometer starts collection of data too soon, t

11 - 25IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.5.7 SituProbe Flow ParameterWARNINGOnly trained users should modify methods. Incorrect

11 - 26 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 11-21 Method Editor Tune Parameter Page

11 - 27IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 11-22 Method Editor Tune Parameter Page - Show Details

11 - 28 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 11-23 Method Editor Tune Report Page

11 - 29IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.7 Full Scan PageWARNINGOnly trained users should modify methods. Changing parameters ma

2 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 2HAPSITE Components and Assemblies2.1 Ship Kit Packing Lists2.2 930-850-G9, G12 Shi

11 - 30 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualStart Mass . . . . . . . . . . . . . . . . . . . . The mass at which the Mass Spectrometer

11 - 31IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.8.1 SIM for Analyze (GC/MS)Figure 11-25 Method Editor SIM Page for Analyze (GC/MS) Ana

11 - 32 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualNOTE: One of the column entries listed above must be highlighted to enable editing of the

11 - 33IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.8.2 SIM for SurveyFigure 11-26 SIM Page, Differences for Survey Analysis

11 - 34 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThe SIM page for Survey mode provides the ability to create only one Scan Set of multiple

11 - 35IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.9 Search PageWARNINGOnly trained users should modify methods. Depending on the search m

11 - 36 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThere are four choices in the Search Mode drop down menu.No Search . . . . . . . . . . . .

11 - 37IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 11-28 AMDIS Search SettingsFigure 11-29 lists the different analysis types availabl

11 - 38 IPN 074-472-P1C HAPSITE Smart Plus Operating Manualretention index standards. In addition to mass spectral data, if the identified compound i

11 - 39IPN 074-472-P1CHAPSITE Smart Plus Operating ManualSensitivity . . . . . . . . . . . . . . . . . . . 1-30, used in model peak perception ran

TrademarksThe trademarks of the products mentioned in this manual are held by the companies that produce them.ConFlat® is a registered trademark of Va

2 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 2-2 930-850-G9, G12 Ship Kit Box 2 ContentsFigure 2-3 930-850-G9, G12 Ship Kit Box

11 - 40 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 11-33 Library OptionsAdvanced SettingsFigure 11-34 Advanced SettingsNOTE: INFICON

11 - 41IPN 074-472-P1CHAPSITE Smart Plus Operating ManualReject Bin . . . . . . . . . . . . . . . . . . . . Rejects peaks with less than set number

11 - 42 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualWriting a quantitative method still begins with Method Editor, but certain buttons will no

11 - 43IPN 074-472-P1CHAPSITE Smart Plus Operating ManualPeak Resolution (dx) . . . . . . . . . . . This number indicates the minimum number of scan

11 - 44 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThe Reset button allows for default values to be reset in the Peak Search window. See Figu

11 - 45IPN 074-472-P1CHAPSITE Smart Plus Operating ManualDisplay. . . . . . . . . . . . . . . . . . . . . . . When enabled, a concentration can be e

11 - 46 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual11.10 Data PageThe Data Page provides the capability to customize the data filenames, and

11 - 47IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFile increment digits. . . . . . . . . . . . This parameter sets the number of digits used

11 - 48 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualData File Path . . . . . . . . . . . . . . . . . The entry box for the data file path is u

11 - 49IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11.11 Summary PageThe Summary Page, see Figure 11-45, provides selections to show any comp

2 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.3 930-850-G10, G11 Ship Kit ContentsThe following items are provided in a typical HAPSITE

11 - 50 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual11.12 How to Create a MethodWARNINGOnly trained users should create methods. Selecting a

11 - 51IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 11-47 Method Editor Open Window3 Choose the method file to be the template for the

11 - 52 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 To save a newly created method from the Method Editor, press the Save button at the bott

11 - 53IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 11-51 Create Folder Button7a If creating a new folder, name the new folder and then

11 - 54 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Type a new name for the sequenced method or use the name provided. See Figure 11-54.NOTE

11 - 55IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 Choose a method file to add to the sequence. Click OK. See Figure 11-55.Figure 11-55 Cho

11 - 56 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual6 Repeat Step 4 and Step 5 until all desired methods are listed in the Method Run List. Se

11 - 57IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 11-57 Saving Sequenced Method

11 - 58 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

12 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 12Target Compound Methods12.1 Introduction To Quantitative AnalysisQuantitative ana

2 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 2-6 930-850-G10, G11 Ship Kit Box 2 ContentsFigure 2-7 930-850-G10, G11 Ship Kit Bo

12 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual12.2 Definition of Terms in the Calibrate WindowFigure 12-1 Calibrate Window12.2.1 Metho

12 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating ManualDisplay. . . . . . . . . . . . . . . . . . . . . . . Displays the chromatogram for the selec

12 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual12.2.4 AnalytesAnalytes in Library. . . . . . . . . . . . . Displays the analytes in the l

12 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating ManualArea . . . . . . . . . . . . . . . . . . . . . . . . . Displays the integrated analyte area

12 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual12.3 Definition of Terms in the ID Unknowns WindowFigure 12-4 ID Unknowns Window12.3.1 M

12 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual12.3.3 Peak SearchSearch . . . . . . . . . . . . . . . . . . . . . . . Performs a peak dete

12 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualCompound . . . . . . . . . . . . . . . . . . . Shows the compound name found in AMDIS, NIS

12 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual12.4 Display FunctionThe Display button in the Data Files section of both Calibrate and ID

12 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating Manualbe added, place the cursor in the mass spectrum window and click the right mouse button to

12 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2 After the standard(s) have been prepared, a method must be developed to collect the data.

2 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.3.1 Ship Kits Box 3 and 4Figure 2-9 USA 24V Power Supply (AC To DC Power Converter) - Box

12 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 12-10 Accessing the Calibrate Function3a Selecting the Calibrate function will dis

12 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 12-11 Selecting the Type of Quantitative Method3b Click OK.3c The Method File windo

12 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualCompound names and CAS#’s. See Figure 12-13. The Chromatogram display window will automati

12 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating ManualDuplicate Row. . . . . . . . . . . . . . Creates a duplicate entry for the highlighted row.

12 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 12-15 Finished Analytes Chart 10d To finish the template, the concentration of eac

12 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 12-17 Save Library Button12 The template is complete and the library is ready for C

12 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 12-19 Calibration Curve12d Additional calibration points can be added to the curve

12 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 12-20 Accessing ID Unknowns Function1a Selecting ID Unknowns will display the Selec

12 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 12-22 Sample Quantitation Report

13 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 13Headspace Sampling System13.1 IntroductionThe Headspace Sampling System (HSS) is

2 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.4.1 Attaching the ProbeTo attach the Probe line, plug the LEMO® connector into the port o

13 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual13.1.1 How the HSS OperatesThe function of the HSS is to provide consistent partition of a

13 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manualand moisture from the previous run. During the Purge cycle, the three-way valves change stat

13 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual13.1.4 Consumables RequiredThe following consumables are required for routine analysis whe

13 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating ManualNOTE: Calibration Mixes may be purchased from a variety of laboratory supply businesses in l

13 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual13.2 Using the HAPSITE with HSSThe following instructions can be used as a guideline for s

13 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual13.2.2 Loading the VialsWARNINGWear appropriate Personal Protection Equipment (PPE) as advi

13 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualNOTE: The 40 mL sample vials are intended for one time use only and should be properly disc

13 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating ManualNOTE: Surrogates are used to indicate consistency within the analysis as compared to interna

13 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThe following is a set of examples for amounts of standard mix (at 200 and 2000 g/mL) to

13 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 13-7 Transferring the Sample to a 40 mL Vial7 Label the vial with the appropriate i

2 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.4.2 Remove Exhaust (Vent) CapThe red exhaust (vent) cap is located on the right side of th

13 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualWARNINGDo not insert a vial which is completely full of liquid sample. An adequate airspac

13 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual13.2.4 Cycling the VialsCycling the vials is performed to thermally equilibrate and analyz

13 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual13.3.1 Clean Out after a High Concentration SampleWhen high concentration samples are ana

13 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 13-9 Flush Switch Inside The Headspace Instrument13.3.3 Cleaning the HSS WellsThe

13 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualLoose debris may be removed by turning the HSS upside down with the top door open. (Remove

13 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7 Decontaminate the instrument with a soft cloth and 10% bleach. For decontamination of the

13 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual13.3.6 Replacing The HSS Nitrogen CanisterReplacement of the Nitrogen Canister is on an a

13 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating Manual13.5 Charging the HAPSITE Battery using the HSSHAPSITE batteries may be charged one at a t

13 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

14 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 14SituProbe14.1 SituProbe The SituProbe™ Purge and Trap System is a sampling access

2 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.4.3 Installing the Gas CanistersCAUTIONOnly open the front panel in a dry, uncontaminated

14 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualEach compound will partition according to its solubility in the water phase and its vapor p

14 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual14.4 Operating SpecificationsEnvironmental Temperature . . . . . . . Operating: 5 to 45°C,

14 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual14.5 Consumables 14.5.1 Compressed NitrogenA source of pressurized, ultra high purity Nit

14 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual14.6 Heated ZonesThere are several heated zones that must be maintained when operating the

14 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual14.7 Valves and SequencesThe SituProbe follows a fixed sequence of events to volatilize, t

14 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manuala Concentrator is installed, the HAPSITE’s sampling pathway initially bypasses the Concentra

14 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 14-3 Method Editor Screen for a Default Open Loop MethodFigure 14-4 Purge Tube14.8

14 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual14.9 Background Cleanup14.9.1 IntroductionThe SituProbe / HAPSITE system, with Concentrato

14 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualOpen the SituProbe front door and press the FLUSH switch. The SituProbe will increase the

14 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual The SituProbe Flow Pressure method parameter should be set to supply an excess of a few n

2 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.4.3.1 How to Change or Remove a Gas CanisterPush the lever located on the right of the can

14 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual1c With a stirrer, begin swirling the water. Remove the stirrer and rapidly dispense the s

14 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2 Prepare the standard in volumetric glassware.2a Follow the above procedure for spiking th

14 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 14-6 Figure 6-3. Multi-Point Internal Standard Calibration14.13 MaintenancePeriod

14 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 14-7 Disassembled View of the Sample Collection Tube and Sealing O-RingSample Colle

14 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

15 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 15Service Module15.1 IntroductionThe Service Module (also called the SM) provides s

15 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual15.2 Service Module Input PowerService Modules are available in either 110/220 V(ac) (IPN

15 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual15.3 Components of the Service ModuleThe following section describes the components of both

15 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual15.3.4 Foreline Vent ValveThe Foreline Vent Valve is located in the middle of the MDP/Turb

15 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual15.3.8 Power SupplyThe Service Module Power Supply is a 24 V(dc) supply that provides power

2 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.4.4 Install BatteryInsert the battery by sliding it into the rectangular opening to the

15 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual15.4 When to Use the Service ModuleThe Service Module (SM) can be used with the HAPSITE Ch

15 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual15.5 Plus IQ Software for the Service ModuleThe Plus IQ software for the Service Module can

15 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual15.5.1 The Service Module Tab in Properties WindowFigure 15-7 Service Module Tab in Prope

15 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating ManualConfigure . . . . . . . . . . . . . . . . . . . . Displays control information. See Figure

15 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 15-10 Ion Pump Status WindowTurbo & R.P. Status . . . . . . . . . . . . Displ

15 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating ManualThe following status items are reported in the Service Module tab Properties Window. Refer

15 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualNOTE: If the HAPSITE is already powered on, it does not need to be turned off before placi

15 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual15.7.1 Attaching the HAPSITE to the Service Module using the Plus IQ SoftwareBe sure to co

15 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Double-clicking on the Service Module icon will open the Service Module tab in the HAPSI

15 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating Manual6 When the Attach procedure is finished, the following message will be displayed on the scr

2 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.4.6.1 Connect Laptop with Yellow Crossover CableUnscrew the cap on the port next to the p

15 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 15-20 Accessories4 Touch the ATTACH SM button or using the arrow keys, highlight t

15 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 15-22 Service Model Attached15.8 Detaching the HAPSITEDetaching the HAPSITE allows

15 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Double-clicking on the Service Module icon will open the Service Module tab in the HAPSI

15 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating Manual6 When the Detach procedure is complete, a message will appear confirming a successful deta

15 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualPhysically remove the HAPSITE from the Service Module. Lift the HAPSITE off the Service Mo

15 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating ManualNOTE: Clean any debris or dust from the black rubber o-ring using a lint-free wipe. Wipe th

15 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThe Service Module must be pumped down. Open the Plus IQ program.Double-clicking on the Pu

15 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 15-34 Yellow Protective Cover Placed Over Aluminum Storage Plug on Service ModuleTo

15 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

16 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 16Maintenance16.1 IntroductionThe HAPSITE is designed to require minimal service. R

DECLARATION OF CONFORMITY This is to certify that this equipment, designed and manufactured by: INFICON Inc. Two Technology Pla

2 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.5 Helpful GuidelinesA set of helpful guidelines to keep the HAPSITE safe and operational

16 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual16.2 Safety ConsiderationsWARNINGWhen operating, the NEG Pump is hot! Do not remove when h

16 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual16.3 HAPSITE Symptom - Cause - Remedy ChartTable 16-1 Diagnosing Problems - HAPSITESymptom

16 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4c. Make sure that there is a full unexpired Internal Standard canister in the GC, and make

16 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual9d. Check Turbo Speed in Service Module program. If less then 1480 Hz, Service Module pumps

16 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual18. Retention Time in Chromatograph has drifted. 18a. Unstable carrier gas flow. 18a. Conta

16 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating Manual16.4 Required Environment for General MaintenanceThe HAPSITE is designed for use in the fie

16 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual16.5.1 Contamination of the Mass SpectrometerContamination of the Mass Spectrometer manifo

16 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual16.5.3 Contamination of the Probe and Probe LineContamination of the Probe and Probe Line c

16 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4 With each end of the Probe in a separate hand, alternately move each ends of the Probe L

16 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 16-4 Blow Out Probe Line and Probe with N27 Re-attach the Probe Line to the HAPSITE

2 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.6 HAPSITE ConfigurationsThere are 6 basic configurations for the HAPSITE. The first three

16 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2 Install the 24 V Power electrical cap (P/N 070-1273). See Figure 16-6.3 Install the EXT

16 - 13IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 Install the red exhaust cap (P/N 070-338). See Figure 16-8.6 Install the red N2 inlet cap

16 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual9 Install the red probe cap (P/N 059-0382). See Figure 16-10.10 Install the brass probe no

16 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating Manual16.6 NEG Pump TroubleshootingIf an MS Pressure Warning message is displayed on the front p

16 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 16-13 Service Module Tab

16 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating Manual16.6.1 NEG Pump Bakeout ProcedureA bakeout can be performed with or without the use of the

16 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3 Set the Bakeout Power to 30. The Bakeout Time is usually set to 2 hours. See Figure 16-1

16 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating Manual16.6.2 Reactivating the NEG PumpReactivating the NEG Pump requires having the Service Modu

16 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 16-17 Service Window4 Click the Activate NEG button. 5 At the end of the reactivat

16 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating Manual16.7 NEG Pump Removal, Installation and ActivationDuring boot-up, the HAPSITE will check s

2 - 14 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualTransfer Line (INFICON part number 931-401-P2) — A directional heated line which connects t

16 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual16.7.1 Required Tools and Equipment Service Module (not pictured) Laptop computer (not

16 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating Manual16.7.2 Part 1: NEG Pump Removal1 This procedure requires the use of a Service Module. The

16 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualWARNINGThe NEG Pump becomes very hot when in operation. The software-controlled sequence p

16 - 25IPN 074-472-P1CHAPSITE Smart Plus Operating Manual5 To loosen the chain clamp, turn the nut counter-clockwise until loose. See Figure 16-20Fi

16 - 26 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual16.7.3 Part 2: Service Module Vacuum Interconnect (VI) Valve CleaningWARNINGGloves must b

16 - 27IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3 Wearing safety glasses and gloves, clean the o-ring on the VI valve with methanol. See Fi

16 - 28 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 Replace the VI valve into the bottom of the manifold. Hand tighten. See Figure 16-24.Fig

16 - 29IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7 Place the HAPSITE on the Service Module and lock down with the black side latches. Refer

16 - 30 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2 Remove the new NEG Pump and aluminum gasket from the shipping container. See Figure 16-2

16 - 31IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4 Remove the new NEG Pump from the protective container. See Figure 16-29.CAUTIONThe NEG Pu

2 - 15IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.7.2 Installing the Headspace Sampling SystemRequired PartsThe following items are needed

16 - 32 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual7 Save the rubber “O” ring assembly and container to dispose of the old NEG Pump.8 Place t

16 - 33IPN 074-472-P1CHAPSITE Smart Plus Operating Manual10 Replace the chain clamp insuring that the nut points to the left. Use the torque wrench

16 - 34 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual12 Perform the Attach function by selecting the Attach button on the Service Module tab of

16 - 35IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3 Select default.tun file. See Figure 16-37.Figure 16-37 Select "default.tun" Fi

16 - 36 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual6 Turn off the IS Supply and Tune Feed valves by clicking on the button under each valve.

16 - 37IPN 074-472-P1CHAPSITE Smart Plus Operating Manual9 Click the Right Mouse Button on the X-axis to access the Full Scan Range. See Figure 16-4

16 - 38 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual10 Select Custom. Type 60 in the Start Field and 90 in the End Field. This will enable the

16 - 39IPN 074-472-P1CHAPSITE Smart Plus Operating Manual11 Spray the MicroDuster around the orifices listed below that could be the source of a pos

16 - 40 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual16.7.6 Part 5: Activation of the NEG Pump1 Click on the Service Module tab of the Propert

16 - 41IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4 Select Activate NEG. 5 When prompted on the front panel, enter the Serial Number of the n

2 - 16 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 2-22 Power Supply Y-cable and Back of HSS6 Properly align the labels on the foam in

16 - 42 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualCAUTIONIf the NEG Pump is to be reinstalled, it must be removed when it is at room tempera

16 - 43IPN 074-472-P1CHAPSITE Smart Plus Operating ManualCAUTIONThe NEG pump becomes very hot when in operation. The software-controlled sequence pr

16 - 44 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 To loosen the chain clamp, turn the nut counter-clockwise until loose. See Figure 16-20.

16 - 45IPN 074-472-P1CHAPSITE Smart Plus Operating ManualCAUTIONMake sure all tools are clean by wiping them with methanol on a lint free cloth. Wea

16 - 46 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 16-52 Extension Tube Slid into the Ion Volume13 Use the flat head screw driver to

16 - 47IPN 074-472-P1CHAPSITE Smart Plus Operating Manual18 Tighten the three securing screws with the screw driver. Tighten them alternately and ge

16 - 48 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual4 Using the 1/4" wrench, loosen both 1/4" connection fittings. Note the position

16 - 49IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 16-56 Holding Down the Needle while Tightening the Nuts (So Ferrules Seat Properly)

16 - 50 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual16.10.2 Troubleshooting The Battery Charger16.10.2.1 If No Indicators are IlluminatedThi

17 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 17Glossary17.1 GlossaryAir peak . . . . . . . . . . . . . . . . . . . . . . A respo

2 - 17IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7 The white label THIS END TO ACCESSORY on the insulation should coincide with the white lab

17 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualCarrier Gas . . . . . . . . . . . . . . . . . . . The pure inorganic gas used to aid the fl

17 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating ManualElution time. . . . . . . . . . . . . . . . . . . The time from injection of a specific comp

17 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFull Method . . . . . . . . . . . . . . . . . . . Full method allows the user to specify a

17 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating ManualInlet State . . . . . . . . . . . . . . . . . . . . This refers to a specification of the s

17 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualLibrary . . . . . . . . . . . . . . . . . . . . . . . A user compiled list of compounds, wh

17 - 7IPN 074-472-P1CHAPSITE Smart Plus Operating ManualNIST Library . . . . . . . . . . . . . . . . . . NIST stands for National Institute of Stan

17 - 8 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualRecalculate . . . . . . . . . . . . . . . . . . . An option in the Calibration section of t

17 - 9IPN 074-472-P1CHAPSITE Smart Plus Operating Manual% RSD . . . . . . . . . . . . . . . . . . . . . . . Percent Relative Standard Deviation. Thi

17 - 10 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualSituProbe . . . . . . . . . . . . . . . . . . . . The SituProbe Purge and Trap System is

17 - 11IPN 074-472-P1CHAPSITE Smart Plus Operating ManualTune . . . . . . . . . . . . . . . . . . . . . . . . . A term (noun or verb) which generall

2 - 18 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 2-26 This End to HAPSITEFigure 2-27 This End to Headspace9 Connect a pressurized N

17 - 12 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

18 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 18Customer Support18.1 How To Contact Customer SupportWorldwide support information

18 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

19 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 19Part Numbers19.1 HAPSITE Smart Plus System ConfigurationFigure 19-1 HAPSITE Smar

19 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual19.2 HAPSITE Smart Plus Accessories Service Module930-202-G1 . . . . . . . . . . . . . .

19 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual930-4061-G1 . . . . . . . . . . . . . . . . . . Battery Line Insulation931-405-P2. . . . .

19 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualInternal Standard Canisters 930-433-P6. . . . . . . . . . . . . . . . . Canister, Internal

19 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual19.6 Service Module Spare Parts 068-002 . . . . . . . . . . . . . . . . . . . . . . Batter

19 - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

A - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualAppendix AHAPSITE Target CompoundsA.1 Compounds In Order Of Elution Name Formula k Quantio

2 - 19IPN 074-472-P1CHAPSITE Smart Plus Operating Manual10 If using the HSS in portable mode, a battery will need to be installed. Open the front do

A - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

B - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualAppendix BCalibrating Gas MixturesB.1 Acquisition, Preparation, and HandlingWARNINGFailure t

B - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualB.1.1 How to Establish the Desired ConcentrationsThere are two basic ways to obtain several

B - 3IPN 074-472-P1CHAPSITE Smart Plus Operating ManualTransfer fittings should be of the stainless steel Swagelok2 type, and transfer lines should

B - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThere are two basic approaches to assuring that the calibration mix is at atmospheric pressu

B - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manualcontents. The bag should not be filled to the point where the bag appears like a firm "a

B - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualB.1.3 Gas Cylinder Safety, Contamination Checks, and Corrective StepsWARNINGSafety of opera

C - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualAppendix CShipping the HAPSITE and ConsumablesC.1 IntroductionThe HAPSITE instrument and its

C - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manualthe cartons and the paperwork required are exacting and can be tedious, so the easiest appro

C - 3IPN 074-472-P1CHAPSITE Smart Plus Operating ManualThe "Shipper's Declaration for Dangerous Goods" is a "Style F83R" fr

2 - 20 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualNOTE: The aluminum storage plug is supplied with the Service Module. See Figure 2-29.Figure

Index - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualIndexSymbols% RSD 17-9AAC to DC power converter 2-10airleak 16-3, 16-5samples 1-7alignmen

Index - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manualcontamination 14-9, 14-10, 16-7gas chromatograph 16-8probe 16-9symptoms of 16-8curve sta

Index - 3IPN 074-472-P1CHAPSITE Smart Plus Operating ManualHeaters Icon 3-52helium 1-9Help Icon 3-42High Mass 11-38Hot Swap Cable 2-53HSPurge 11-21H

Index - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualMDP/turbo pump 15-3, 15-4accl 15-4norm 15-4speed 15-4Membrane Interface Mass Spectrometr

Index - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manualremotemode 5-1power 17-8repair 16-1Report 10-12calibration 12-4printing 11-25Qualitative

Index - 6 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualTTargetlibrary 6-4Tedlar bag B-4, B-6temperatureramp 11-22Tenax concentrator 11-24thresh

2 - 21IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 2-31 Power Cable Attached at Back Left of the Service ModuleThe RS-232 communication

Immunity: ETSI EN 301 489-17 V1.2.1: 2002 (General EMI) (ERM - EMC - Specific conditions for 2.4 GHz) RoHS: Due to the classific

2 - 22 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 2-33 RS-232 Communication Cable Attached to Back Right Side of Service ModuleAttach

2 - 23IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 2-35 System Setup Screen with Service ModuleNOTE: If the Service Module icon does no

2 - 24 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 2-37 Cleaning the Service Module Rubber O-ring using a Lint-free WipeAfter cleaning

2 - 25IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 2-38 Remove the Yellow Plastic Protective Cover on the Bottom of the HAPSITEFigure 2

2 - 26 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualNOTE: Black latches can be adjusted with the thumb screw to ensure proper tension.Figure 2-

2 - 27IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.9 SituProbeUse the following procedure to set up the SituProbe. For more SituProbe inform

2 - 28 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 The white label THIS END TO ACCESSORY on the insulation should coincide with the white la

2 - 29IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 2-47 Plugging Transfer Line Into HAPSITE and SituProbe7 Open the front panel door of

2 - 30 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 2-49 Purge Vessel Water Flow Direction Shown12 The purge vessel can also be used wi

2 - 31IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.10 Sample Collection ModesThe Sample Loop is used to detect chemicals in the low ppm to h

DECLARATION OF CONFORMITY This is to certify that this equipment, designed and manufactured by: INFICON Inc. Two Technology Place

2 - 32 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 2-52 Tightening the Bottom Nut6 Continue pressing on the top elbow and tighten the

2 - 33IPN 074-472-P1CHAPSITE Smart Plus Operating Manualis applied to the top elbow, the elbow should not slip on the Sample Loop. If the elbow move

2 - 34 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.10.2 Removing the Sample LoopCAUTIONTo prevent contamination, only open front panel in a

2 - 35IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 2-56 Proper Tri-Bed Concentrator OrientationNOTE: The Tenax Concentrator does not ha

2 - 36 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual3a For the Tenax Concentrator: While holding the nut and ferrule in place, carefully place

2 - 37IPN 074-472-P1CHAPSITE Smart Plus Operating Manual4 For the Tri-Bed Concentrator: Carefully lift up on the top elbow fitting and insert the en

2 - 38 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 Keep the Concentrator aligned between the two elbow fittings while gently pressing down o

2 - 39IPN 074-472-P1CHAPSITE Smart Plus Operating ManualWARNINGExcessive force and/or tightening can cause the fragile glass to break!7 When pressur

2 - 40 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualFigure 2-63 Installed Concentrator CoverNOTE: If the cover does not easily fit over the Co

2 - 41IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 2-65 Back of the Old Concentrator Cover9 Close the front panel.2.10.4 Removing the

CE Implementation Date: March 31, 2006 Authorized Representative: Duane H. Wright Operations Quality Manager, ISS INFICON Inc.

2 - 42 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.11 Probe Sampling Options and AttachmentsTo expand the sampling range of the HAPSITE, sa

2 - 43IPN 074-472-P1CHAPSITE Smart Plus Operating ManualFigure 2-66 Diagram of Proper Ferrule Orientation in the Probe Nut2.11.2 Attaching a Bag S

2 - 44 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.11.3 VX / R-33 Conversion TubeThis procedure describes the steps required to prepare the

2 - 45IPN 074-472-P1CHAPSITE Smart Plus Operating Manual3 Insert either end of the VX / R-33 Conversion Tube into the nut. Make sure the tube is fir

2 - 46 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.11.3.2 VX / R-33 Conversion Tube RemovalWARNINGIf conversion tube has been exposed take

2 - 47IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.12 BatteriesThe battery provides power to the HAPSITE to allow portability. Under optimum

2 - 48 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.12.2 Battery ChargerThe auxiliary Battery Charger (part number 930-470-G1—see Figure 2-7

2 - 49IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.12.2.1 Battery Charger ComponentsThe Battery Charger is shipped with a power cord and spa

2 - 50 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.12.2.4 Understanding the Battery Charger IndicatorsEach battery receptacle is associated

2 - 51IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.13 Portable AccessoriesPortability is an important HAPSITE feature. The following accesso

DECLARATION OF CONFORMITY This is to certify that this equipment, designed and manufactured by: INFICON Inc. Two Technology Place

2 - 52 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual2.13.2 HAPSITE BackpackThe backpack is a light weight, high quality hiker’s backpack. It h

2 - 53IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.13.2.2 Care of the Backpack Avoid exposing the backpack to solvents and other active che

2 - 54 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualWARNING - Risk Of Electric ShockDo not use if the "L" connector is broken. WARNIN

2 - 55IPN 074-472-P1CHAPSITE Smart Plus Operating Manual2.14.2 Storing the Hot Swap CableThe Hot Swap Cable and Battery have exposed electrical con

2 - 56 IPN 074-472-P1C HAPSITE Smart Plus Operating ManualThis page is intentionally blank.

3 - 1IPN 074-472-P1CHAPSITE Smart Plus Operating ManualChapter 3Operating HAPSITE in Portable Mode3.1 Starting the HAPSITE in Portable ModePortable

3 - 2 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual5 During the preparation period, the front panel will display the PREPARING SYSTEM message.

3 - 3IPN 074-472-P1CHAPSITE Smart Plus Operating Manual7 The progress of the preparation is shown by a bar graph. If a component is in the process o

3 - 4 IPN 074-472-P1C HAPSITE Smart Plus Operating Manual11 When the HAPSITE is ready to run samples, a green SYSTEM READY, SURVEY READY or ANALYZE R

3 - 5IPN 074-472-P1CHAPSITE Smart Plus Operating Manual12 If SURVEY READY is displayed, touch RUN SURVEY or push SURVEY RUN. See Figure 3-7Figure 3-